Novel acrylamide assisted polymeric citrate route for the synthesis of nanocrystalline ZrO2 powders for dental applications

S. Vivekanandhan, M. Venkateswarlu, H. R. Rawls, N. Satyanarayana

Resultado de la investigación: Conference contribution

Resumen

The acrylamide assisted polymeric citrate route was investigated for the synthesis of nanocrystalline ZrO2 powders, using zirconium oxychloride as the source for metal ion along with citric acid and acrylamide as chelating as well as polymerizing agents. The complete process for the synthesis of nanocrystalline ZrO2 powders was monitored by TG/DTA, FTIR, XRD and TEM techniques. Thermal decomposition of the polymeric intermediate was investigated using TG/DTA analysis. Structural coordination and phase of the synthesized ZrO2 powders were investigated by FTIR and XRD analysis respectively. The microstructure of the synthesized nanocrystalline ZrO2 powder was identified using transmission electron microscopy, which showed -lOnm agglomerates of still finer ZrO2 particles.

Idioma originalEnglish (US)
Título de la publicación alojada2007 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2007, Technical Proceedings
Páginas293-296
Número de páginas4
EstadoPublished - 2007
Evento2007 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2007 - Santa Clara, CA, United States
Duración: may 20 2007may 24 2007

Serie de la publicación

Nombre2007 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2007, Technical Proceedings
Volumen4

Other

Other2007 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2007
País/TerritorioUnited States
CiudadSanta Clara, CA
Período5/20/075/24/07

ASJC Scopus subject areas

  • Mechanical Engineering

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