Synthesis of nanocrystallinc ZrO2 powder by the polyol route

S. Vivekanandhan; M. Venkateswarlu; H. R. Rawls; N. Satyanarayana

Synthesis of nanocrystallinc ZrO₂ powder by the polyol route

S. Vivekanandhan, M. Venkateswarlu, H. R. Rawls, N. Satyanarayana

Comprehensive Dentistry

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution

1 Scopus citations

Abstract

The polyol route, with zirconium oxychloridc as the metal ion source, was used to synthesize nanocrystallinc ZrO₂ powder. The complete process for the synthesis of nanocrystallinc ZrO₂ was monitored by TG/DTA, FTIR. XRD and TEM. Thermal behavior of the intermediate powder was investigated using TG/DTA analysis. The structural coordination and phase of the intermediate, as well as the synthesized ZrO₂ powder, were investigated by FTIR and XRD respectively. The microstructure of the synthesized nanocrystallinc ZrO₂ powder was identified using transmission electron microscopy.

Original language	English (US)
Title of host publication	Nanotechnology 2009
Subtitle of host publication	Fabrication, Particles, Characterization, MEMS, Electronics and Photonics - Technical Proceedings of the 2009 NSTI Nanotechnology Conference and Expo, NSTI-Nanotech 2009
Pages	125-128
Number of pages	4
State	Published - 2009
Event	Nanotechnology 2009: Fabrication, Particles, Characterization, MEMS, Electronics and Photonics - 2009 NSTI Nanotechnology Conference and Expo, NSTI-Nanotech 2009 - Houston, TX, United States Duration: May 3 2009 → May 7 2009

Publication series

Name	Nanotechnology 2009: Fabrication, Particles, Characterization, MEMS, Electronics and Photonics - Technical Proceedings of the 2009 NSTI Nanotechnology Conference and Expo, NSTI-Nanotech 2009
Volume	1

Other

Other	Nanotechnology 2009: Fabrication, Particles, Characterization, MEMS, Electronics and Photonics - 2009 NSTI Nanotechnology Conference and Expo, NSTI-Nanotech 2009
Country	United States
City	Houston, TX
Period	5/3/09 → 5/7/09

Keywords

Nanocrystallinc ZrO powder
Polyol synthesis: TG/DTA: FTIR
TEM
XRD

ASJC Scopus subject areas

Electrical and Electronic Engineering
Electronic, Optical and Magnetic Materials
Condensed Matter Physics

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Vivekanandhan, S., Venkateswarlu, M., Rawls, H. R., & Satyanarayana, N. (2009). Synthesis of nanocrystallinc ZrO₂ powder by the polyol route. In Nanotechnology 2009: Fabrication, Particles, Characterization, MEMS, Electronics and Photonics - Technical Proceedings of the 2009 NSTI Nanotechnology Conference and Expo, NSTI-Nanotech 2009 (pp. 125-128). (Nanotechnology 2009: Fabrication, Particles, Characterization, MEMS, Electronics and Photonics - Technical Proceedings of the 2009 NSTI Nanotechnology Conference and Expo, NSTI-Nanotech 2009; Vol. 1).

Synthesis of nanocrystallinc ZrO₂ powder by the polyol route. / Vivekanandhan, S.; Venkateswarlu, M.; Rawls, H. R.; Satyanarayana, N.

Nanotechnology 2009: Fabrication, Particles, Characterization, MEMS, Electronics and Photonics - Technical Proceedings of the 2009 NSTI Nanotechnology Conference and Expo, NSTI-Nanotech 2009. 2009. p. 125-128 (Nanotechnology 2009: Fabrication, Particles, Characterization, MEMS, Electronics and Photonics - Technical Proceedings of the 2009 NSTI Nanotechnology Conference and Expo, NSTI-Nanotech 2009; Vol. 1).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution

Vivekanandhan, S, Venkateswarlu, M, Rawls, HR & Satyanarayana, N 2009, Synthesis of nanocrystallinc ZrO₂ powder by the polyol route. in Nanotechnology 2009: Fabrication, Particles, Characterization, MEMS, Electronics and Photonics - Technical Proceedings of the 2009 NSTI Nanotechnology Conference and Expo, NSTI-Nanotech 2009. Nanotechnology 2009: Fabrication, Particles, Characterization, MEMS, Electronics and Photonics - Technical Proceedings of the 2009 NSTI Nanotechnology Conference and Expo, NSTI-Nanotech 2009, vol. 1, pp. 125-128, Nanotechnology 2009: Fabrication, Particles, Characterization, MEMS, Electronics and Photonics - 2009 NSTI Nanotechnology Conference and Expo, NSTI-Nanotech 2009, Houston, TX, United States, 5/3/09.

Vivekanandhan S, Venkateswarlu M, Rawls HR, Satyanarayana N. Synthesis of nanocrystallinc ZrO₂ powder by the polyol route. In Nanotechnology 2009: Fabrication, Particles, Characterization, MEMS, Electronics and Photonics - Technical Proceedings of the 2009 NSTI Nanotechnology Conference and Expo, NSTI-Nanotech 2009. 2009. p. 125-128. (Nanotechnology 2009: Fabrication, Particles, Characterization, MEMS, Electronics and Photonics - Technical Proceedings of the 2009 NSTI Nanotechnology Conference and Expo, NSTI-Nanotech 2009).

Vivekanandhan, S. ; Venkateswarlu, M. ; Rawls, H. R. ; Satyanarayana, N. / Synthesis of nanocrystallinc ZrO₂ powder by the polyol route. Nanotechnology 2009: Fabrication, Particles, Characterization, MEMS, Electronics and Photonics - Technical Proceedings of the 2009 NSTI Nanotechnology Conference and Expo, NSTI-Nanotech 2009. 2009. pp. 125-128 (Nanotechnology 2009: Fabrication, Particles, Characterization, MEMS, Electronics and Photonics - Technical Proceedings of the 2009 NSTI Nanotechnology Conference and Expo, NSTI-Nanotech 2009).

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abstract = "The polyol route, with zirconium oxychloridc as the metal ion source, was used to synthesize nanocrystallinc ZrO2 powder. The complete process for the synthesis of nanocrystallinc ZrO2 was monitored by TG/DTA, FTIR. XRD and TEM. Thermal behavior of the intermediate powder was investigated using TG/DTA analysis. The structural coordination and phase of the intermediate, as well as the synthesized ZrO2 powder, were investigated by FTIR and XRD respectively. The microstructure of the synthesized nanocrystallinc ZrO2 powder was identified using transmission electron microscopy.",

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note = "Copyright: Copyright 2009 Elsevier B.V., All rights reserved.; Nanotechnology 2009: Fabrication, Particles, Characterization, MEMS, Electronics and Photonics - 2009 NSTI Nanotechnology Conference and Expo, NSTI-Nanotech 2009 ; Conference date: 03-05-2009 Through 07-05-2009",

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