Synthesis of nanocrystallinc ZrO2 powder by the polyol route

S. Vivekanandhan, M. Venkateswarlu, H. R. Rawls, N. Satyanarayana

Research output: Chapter in Book/Report/Conference proceedingConference contribution

1 Scopus citations

Abstract

The polyol route, with zirconium oxychloridc as the metal ion source, was used to synthesize nanocrystallinc ZrO2 powder. The complete process for the synthesis of nanocrystallinc ZrO2 was monitored by TG/DTA, FTIR. XRD and TEM. Thermal behavior of the intermediate powder was investigated using TG/DTA analysis. The structural coordination and phase of the intermediate, as well as the synthesized ZrO2 powder, were investigated by FTIR and XRD respectively. The microstructure of the synthesized nanocrystallinc ZrO2 powder was identified using transmission electron microscopy.

Original languageEnglish (US)
Title of host publicationNanotechnology 2009
Subtitle of host publicationFabrication, Particles, Characterization, MEMS, Electronics and Photonics - Technical Proceedings of the 2009 NSTI Nanotechnology Conference and Expo, NSTI-Nanotech 2009
Pages125-128
Number of pages4
StatePublished - Nov 26 2009
EventNanotechnology 2009: Fabrication, Particles, Characterization, MEMS, Electronics and Photonics - 2009 NSTI Nanotechnology Conference and Expo, NSTI-Nanotech 2009 - Houston, TX, United States
Duration: May 3 2009May 7 2009

Publication series

NameNanotechnology 2009: Fabrication, Particles, Characterization, MEMS, Electronics and Photonics - Technical Proceedings of the 2009 NSTI Nanotechnology Conference and Expo, NSTI-Nanotech 2009
Volume1

Other

OtherNanotechnology 2009: Fabrication, Particles, Characterization, MEMS, Electronics and Photonics - 2009 NSTI Nanotechnology Conference and Expo, NSTI-Nanotech 2009
CountryUnited States
CityHouston, TX
Period5/3/095/7/09

Keywords

  • Nanocrystallinc ZrO powder
  • Polyol synthesis: TG/DTA: FTIR
  • TEM
  • XRD

ASJC Scopus subject areas

  • Electrical and Electronic Engineering
  • Electronic, Optical and Magnetic Materials
  • Condensed Matter Physics

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