Novel acrylamide assisted polymeric citrate route for the synthesis of nanocrystalline ZrO2 powders for dental applications

S. Vivekanandhan, M. Venkateswarlu, H. R. Rawls, N. Satyanarayana

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Abstract

The acrylamide assisted polymeric citrate route was investigated for the synthesis of nanocrystalline ZrO2 powders, using zirconium oxychloride as the source for metal ion along with citric acid and acrylamide as chelating as well as polymerizing agents. The complete process for the synthesis of nanocrystalline ZrO2 powders was monitored by TG/DTA, FTIR, XRD and TEM techniques. Thermal decomposition of the polymeric intermediate was investigated using TG/DTA analysis. Structural coordination and phase of the synthesized ZrO2 powders were investigated by FTIR and XRD analysis respectively. The microstructure of the synthesized nanocrystalline ZrO2 powder was identified using transmission electron microscopy, which showed -lOnm agglomerates of still finer ZrO2 particles.

Original languageEnglish (US)
Title of host publication2007 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2007, Technical Proceedings
Pages293-296
Number of pages4
StatePublished - Aug 23 2007
Event2007 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2007 - Santa Clara, CA, United States
Duration: May 20 2007May 24 2007

Publication series

Name2007 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2007, Technical Proceedings
Volume4

Other

Other2007 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2007
CountryUnited States
CitySanta Clara, CA
Period5/20/075/24/07

Keywords

  • Acrylamide
  • Combustion
  • FTIR
  • Nanocrystalline ZrO
  • TEM
  • TG/DTA
  • XRD

ASJC Scopus subject areas

  • Mechanical Engineering

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    Vivekanandhan, S., Venkateswarlu, M., Rawls, H. R., & Satyanarayana, N. (2007). Novel acrylamide assisted polymeric citrate route for the synthesis of nanocrystalline ZrO2 powders for dental applications. In 2007 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2007, Technical Proceedings (pp. 293-296). (2007 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2007, Technical Proceedings; Vol. 4).